PES多孔材料的制备与表征.PDFVIP

Studies in Synthetic Chemistry 合成化学研究, 2017, 5(3), 20-28 Published Online September in Hans. /journal/ssc /10.12677/ssc.2017.53004 Preparation and Characterization of Polyethersulfone (PES) Porous Materials Zhuo Ni, Peifang Lin, Sha Yang, Zeyu Lin College of Chemistry and Environmental Engineering, Shenzhen University, Shenzhen Guangdong th th th Received: Jul. 28 , 2017; accepted: Aug. 11 , 2017; published: Aug. 18 , 2017 Abstract Dimethylacetamide (DMF) was used as the solvent to dissolve the polymer, and then mixed with the treated sodium chloride (NaCl) porogen granules. The polymer/sodium chloride (NaCl) mate- rials were prepared by casting method. The PES porous materials were extracted with deionized water to study the pore structure, porosity and water absorption of PES. Using the same particle size porogen, the water absorption of the PES pore material increases with the amount of porogen, but when the mass ratio of PES and porogen is more than a certain degree, the water absorption decreased. The water absorption of the PES pore material was not linearly related to the size of the pore structure using three porosens of different particle sizes. The PES pore structure was characterized by optical microscopy and scanning electron microscopy. It was found that the ma- terial was a three-dimensional porous material with inter-pore connectivity. Keywords Polyethersulfone (PES), Porogen, Pore Material, Pore Structure, Water Absorption 聚醚砜(PES)多孔材料的制备与表征 倪 卓，林佩芳，杨 莎，林泽宇 深圳大学化学与环境工程学院，广东 深圳 收稿日期：2017年7月28 日；录用日期：2017年8月11 日；发布日期：2017年8月18 日 文章引用: 倪卓, 林佩芳, 杨莎, 林泽宇. 聚醚砜(PES)多孔材料的制备与表征[J]. 合成化学研究, 2017, 5(3): 20-28. DOI: 10.12677/ssc.201