烧结制度对钙长石质耐火材料显微结构影响.pdfVIP

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烧结制度对钙长石质耐火材料显微结构影响.pdf

Material Sciences 材料科学, 2012, 2, 83-88 doi:10.4236/ms.2012.22015 Published Online April 2012 (/journal/ms) The Influences of Sintering Systems on Microstructure of Anorthite Light Heat Insulation Refractory Materials 1 1 1* 2 Furong Feng , Yuesheng Chai , Yuming Tian , Yuxing Qin 1MgMg-Alloy Engineering Technology Research Center, Taiyuan University of Science and Technology, Taiyuan 2State Intellectual Property Office, Beijing * Email: tianyming@163.com Received: Dec. 31st, 2011; revised: Jan. 19th, 2012; accepted: Jan. 26th, 2012 Abstract: The magnesium slag, kaolin and alumina as raw material, sinter anorthite lightweight insulating refractory. The paper studied firing temperature and holding time affecting the sample microstructures. The results showed that: the new crystalline phases are mainly anorthite and alumina. With increasing temperature, grains increases which are mainly plate-like bodies and cylindrical bodies. At the same time, with the temperature grains grow up from 1 μm to 10 μm, aggregates increases, porosity increases and isolated. 1350˚C - 1370˚C are the appropriate sintering temperatures with grains size in the 2 - 5 μm, volume density 1.52 g/cm3 and the rate of open pores 60%. In 1370˚C temperature, with holding time changing, grains size does not change after the 5 μm, but the bond formed by the aggregate grains gradually from large to small and uniformity, along with uniform pores, volume density 1.50 - 1.53 g/cm3 and the rate of open pores 57% - 60%. Keywords: Anorthite; Sintering Temperature; Holding Time; Microstructure 烧结制度对钙长石质耐火

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