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薄层扫描法测定通脉口服液中葛根素含量(Determination of Puerarin in Tongmai oral liquid by TLC scanning)
薄层扫描法测定通脉口服液中葛根素含量(Determination of Puerarin in Tongmai oral liquid by TLC scanning)
Determination of Puerarin in Tongmai oral liquid by TLC scanning
Update Date: 2010-06-08 Click: Ma Hantao
Abstract: the content of Puerarin in Tongmai oral liquid was determined by TLC scanning. The average recovery rate was 97.13% (n=6), RSD=2.65%. The method was simple, specific, sensitive and reproducible.
Keywords Tongmai oral liquid; puerarin; TLC scanning; content determination;
Determination, of, Puerarin, in, Tongmai, Oral, Solution, by, TLCS
Ma Hantao
Affiliated, Hospital, of, Luoyang, Medical, College, Luoyang 471003
Abstract, TLCS, was, used, to, Puerarin, in, Tongmai, solution., The, average, recovery, was, oral (n=6), and, the, RSD, was, 2.65%.,, Alismol, was,, efficiently, determine, quantitated, by, TLCS.
Key, words, Tongmai, oral, solution; Puerarin; TLCS; Determination
Tongmai oral liquid is a new preparation for the treatment of cardiovascular and cerebrovascular diseases. It is mainly composed of Pueraria lobata and other traditional Chinese medicine. Radix puerariae is the main prescription and its effective component is puerarin. Root of kudzu, Pueraria lobata two varieties. Ref. 1 reports, significantly higher than the content of Puerarin in Pueraria lobata pueraria. In order to ensure the clinical efficacy of the preparation, selection of feed production of Pueraria lobata. In order to control the quality of the preparation, the content of Puerarin in the preparation was determined by TLC scanning.
1 instrument and reagent
CS-930 IPC dual wavelength flying spot scanner (Shimadzu Corporation), trace quantitative capillary (Drummond, Co.) 939 thin plate making device for (the South Bank of Chongqing Baird instrument factory); Ge Gensu (provided by the China control of pharmaceutical and biological products), silica gel G (for Qingdao ocean chemical industry group company), the reagents used are the analysis of pure.
2 preparation of reference solution and test s
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