分析天平校正与使用SOP.pdf

SOP No. 2110 Rev 11 Title: Calibration and Use of Analytical Balances Filename: 2110v11.lwp Reference: Current version USP. Rev. No. Date Revised Revision Summary 1. 09-06-91 Original SOP 2. 10-25-91 Weight for calibration of semimicro balance changed to 2 g 3. 09-30-93 New Format 4. 12-09-93 Added CLP Requirements 5. 12-14-94 Minor revisions, 5.2: re-certification of 1 and 50 g Class S weights 6. 12-17-97 for 2 weeks deleted from 5.1 and OOS investigation added 7. 07-08-98 5.1 The QAU responsible for both re-calibration of balances if results exceed control limits as well as coordination of balance inspections by an outside service. The results from weekly weighings are documented in the QA Logbook instead of on 3 X 5” cards, and personnel responsible for conducting weekly checks updated. 8. 12-06-99 Changed to current SOP format. 5.1: semi-micro checked with additional 10 or 20 mg weight. 5.1.1.2: added 9. 05-01-00 Sec 1.0, 2.0, 3.0: scope widened to include use of balances. Sec. 4.1, 5.0: added. 10. 02-21-02 Sec. 2.0: Changed balance check from weekly to daily, changed reference form Sec.5.2 to 5.0 and added reference to Sec. 6.0. Section 6.1: Added check with 50g weight remainder of week.