明德验表述hj.pdfVIP

Sentence Template for Notebook and Report Writing WuXi PharmaTech Co., Ltd. Sentence Template for Notebook and Report Writing Pfizer Project Management Team April 12, 2007 Part 1: 反应前的装置描述 1.1: A 3 L three-necked round bottom flask equipped with mechanical stirrer (or magnetic stirrer), addition funnel and thermometer (or Dean-Stock; drying tube) 1.2: All flasks used in the reaction were heated under vacuum for 30 minutes and purged with N for 10 minutes. (无水反应装置) 2 Part 2: 加料 2.1: 不同的顺序和表达 2.1.1: A 3 L three-necked round bottom flask equipped with mechanical stirrer (or magnetic stirrer), addition funnel and thermometer (or Dean-Stock; drying tube) were charged with A (10 mL, 1 mole), B (2 g, mole) and C (50 mL), 2.1.1.1: a solution of D (10 g, 1 mole) in E (20 mL) was added dropwise (via addition funnel or syringe) at 10oC (or while maintaining gentle reflux; while keeping inner temperature o o between 10 C – 30 C) under N2 （液体滴加到反应液中） 2.1.1.2: D (10 g, 1 mole) was added in portions during a period of 1 hr ( 固体分批加入到反 应液中) 2.1.1.3: D (10 g, 1 mole) and E (20 mL) were added in turn 2.2: To a solution (mixture, suspension or slurry) of A (10 mL, 1 mole) and B (2 g, mole) in C (50 mL) 2.2.1: was added dropwise a solution of D (10 g, 1 mole) in E (20 mL) with stirring at 10oC (or while maintaining gentle reflux; while keeping inner temperature between 10o o C – 30 C) under N2 2.2.2: was added D (10 g, 1 mole) in portions during a period of 1 hr Confidential Page 1 of 7 Sentence Template for Notebook and Report Writing WuXi PharmaTech Co., Ltd. 2.2.3: we