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Basics of X-Ray Powder Diffraction Self-User Training for the…
Basics of X-Ray Powder Diffraction ;Training Required to become an Independent User in the X-Ray Shared Experimental Facility at the Center for Materials Science and Engineering at MIT;Required Safety Training;Instrument Specific Training ;Data Analysis Workshops;High Resolution X-Ray Diffraction (HRXRD) Training;Introduction to Crystallography and X-Ray Diffraction Theory;2012 was the 100th Anniversary of X-Ray Diffraction;The Laue diffraction pattern ;An X-ray powder diffraction pattern is a plot of the intensity of X-rays scattered at different angles by a sample ;X-rays scatter from atoms in a material and therefore contain information about the atomic arrangement;Diffraction occurs when light is scattered by a periodic array with long-range order, producing constructive interference at specific angles.;Crystalline materials are characterized by the long-range orderly periodic arrangements of atoms.;The diffraction pattern is a product of the unique crystal structure of a material ;Diffraction pattern calculations treat a crystal as a collection of planes of atoms;A Brief Introduction to Miller Indices;The diffraction peak position is a product of interplanar spacing, as calculated by Bragg’s law;The diffraction peak intensity is determined by the arrangement of atoms in the entire crystal;Bragg’s law provides a simplistic model to understand what conditions are required for diffraction. ;Many powder diffractometers use the Bragg-Brentano parafocusing geometry.;A single crystal specimen in a Bragg-Brentano diffractometer would produce only one family of peaks in the diffraction pattern.;;Powder diffraction is more aptly named polycrystalline diffraction;X-rays are scattered in a sphere around the sample;X-Ray Powder Diffraction (XRPD) is a somewhat inefficient measurement technique;Diffraction patterns are collected as absolute intensity vs 2q, but are best reported as relative intensity vs dhkl.;Powder diffraction data consists of a record of photon intens
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