- 1、本文档共107页,可阅读全部内容。
- 2、原创力文档(book118)网站文档一经付费(服务费),不意味着购买了该文档的版权,仅供个人/单位学习、研究之用,不得用于商业用途,未经授权,严禁复制、发行、汇编、翻译或者网络传播等,侵权必究。
- 3、本站所有内容均由合作方或网友上传,本站不对文档的完整性、权威性及其观点立场正确性做任何保证或承诺!文档内容仅供研究参考,付费前请自行鉴别。如您付费,意味着您自己接受本站规则且自行承担风险,本站不退款、不进行额外附加服务;查看《如何避免下载的几个坑》。如果您已付费下载过本站文档,您可以点击 这里二次下载。
- 4、如文档侵犯商业秘密、侵犯著作权、侵犯人身权等,请点击“版权申诉”(推荐),也可以打举报电话:400-050-0827(电话支持时间:9:00-18:30)。
查看更多
Basics of X-Ray Powder Diffraction Self-User Training for the…
Basics of X-Ray Powder Diffraction;Training Required to become an Independent User in the X-Ray Shared Experimental Facilityat the Center for Materials Science and Engineering at MIT;Required Safety Training;Instrument Specific Training ;Data Analysis Workshops;High Resolution X-Ray Diffraction (HRXRD) Training;Introduction to Crystallography and X-Ray Diffraction Theory;2012 was the 100th Anniversary of X-Ray Diffraction;The Laue diffraction pattern ;An X-ray powder diffraction pattern is a plot of the intensity of X-rays scattered at different angles by a sample ;X-rays scatter from atoms in a material and therefore contain information about the atomic arrangement;Diffraction occurs when light is scattered by a periodic array with long-range order, producing constructive interference at specific angles.;Crystalline materials are characterized by the long-range orderly periodic arrangements of atoms.;The diffraction pattern is a product of the unique crystal structure of a material ;Diffraction pattern calculations treat a crystal as a collection of planes of atoms;A Brief Introduction to Miller Indices;The diffraction peak position is a product of interplanar spacing, as calculated by Bragg’s law;The diffraction peak intensity is determined by the arrangement of atoms in the entire crystal;Bragg’s law provides a simplistic model to understand what conditions are required for diffraction. ;Many powder diffractometers use the Bragg-Brentano parafocusing geometry.;A single crystal specimen in a Bragg-Brentano diffractometer would produce only one family of peaks in the diffraction pattern.;;Powder diffraction is more aptly named polycrystalline diffraction;X-rays are scattered in a sphere around the sample;X-Ray Powder Diffraction (XRPD) is a somewhat inefficient measurement technique;Diffraction patterns are collected as absolute intensity vs 2q, but are best reported as relative intensity vs dhkl.;Powder diffraction data consists of a record of photon intens
文档评论(0)