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Laser Ablation ICP-MS of Siderophile and Chalcophile Elements 激光烧蚀ICP-MS的亲铁和硫元素
Laser Ablation ICP-MS of Siderophile and Chalcophile Elements in Mid-Oceanic Ridge Glasses Evelyn Martinique Mervine Dartmouth College July 29th, 2005 Mentor: Dr. Vincent Salters, Geochemistry Outline Goals of the Study Background Sample Selection and Analysis Data Conclusions Acknowledgements Goals of the Study Develop technique for measuring siderophile and chalcophile elements in glasses Compare LA-ICP-MS with traditional ICP-MS Examine residual aprons Study how siderophile and chalcophile elements behave during crystal fractionation Background: Goldschmidt’s Classification of the Elements Atmophile: Noble gases Covalently-bonded gases Siderophile: Metals near and including iron in the periodic table Transition metals Exhibit metallic bonding Chalcophile: Elements that bond to S, Se, Te, Sb, and As Tend to form covalent bonds Lithophile: Elements which typically bond to oxygen in silicates and oxides Tend to form ionic bonds Background: Why Study Siderophile and Chalcophile Elements? Scientists do not understand the behavior of most siderophile and chalcophile elements well Can compare behavior of siderophile and chalcophile elements during magma genesis with the well-known behavior of major and other trace elements What these elements may tell us: Oxidation state of the mantle Behavior of sulfur during magma genesis Composition of the Earth’s core Sample Selection Mid-Atlantic Ridge Glasses On loan from Smithsonian’s Volcanic Glass Collection Thirty samples, divided into two suites of fifteen Each suite represents samples related through crystal fractionation Indian Ridge Glasses Already at the lab Used for method development Analysis Glass chips mounted in epoxy on a slide Slide polished to reveal flat glass surface Slide placed in sample holder Laser beam fired on sample, ablates sample Sample flows to the Finnigan ICP-MS, which ionizes the sample Elemental concentrations measured by separating ions based on mass in a magnetic field and counting
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