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Inert Gas Purification Systems - Vacuum Atmospheres Company：惰性气体净化系统-真空环境公司
Inert Gas Purification Systems Why do we need them??? Many of the materials used in research and development today are extremely air sensitive, and can be dangerous in the presence of air. Purifiers are designed to remove oxygen, moisture and nitrogen/hydrogen from an inert gas to one part per million. Safety is also a critical issue in experiments and research today. Purifier Components Circulation blower Copper catalyst Molecular Sieve Vacuum pump Solenoid Assembly Pressure control Regeneration control Manual footswitch Isolation valves (automatic or manual) Solvent removal systems Titanium reactor (in the case of N2/H2 removal) Exhaust traps Purifier theory The purpose of a purifier is to remove oxygen and water from an inert gas flowing through a controlled atmosphere system such as a glove-box. The typical purifier contains two purification agents. One agent is a molecular sieve that removes water by the process of molecular adsorption.The other agent is called Q5 and is an oxygen reactant material. Oxygen removal Oxygen removal from argon, helium, or nitrogen is accomplished with a reactant/catalyst known as Q5, a material consisting of finely divided copper on an alumina matrix. The copper reacts with oxygen to form copper (II) oxide. Moisture removal Moisture is removed by a molecular sieve enclosed in the same container as the oxygen reactant. Also removed by the molecular sieve at ambient temperatures are carbon dioxide, nitrogen dioxide, hydrogen sulfide, carbon monoxide and many organic compounds including: Alcohols, aromatics, amines, halogenated compounds, oxygenated compounds, hydrocarbons and organic acids. Regeneration Theory To restore the purification capability of the material two reactions must take place. The H2O trapped by the sieve must be removed completely. The O2 must be removed from the Q5 reactant by reduction using hydrogen and heat. Regeneration theory (cont.) The restoration of the sieve is accomplished by heating the materi
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