三电参数对铝合金微弧氧化陶瓷膜封孔的影响.PDFVIP

20 13 年 电 工 技 术 学 报 Vol.2 8 Sup.1 第28 卷增刊 1 TRANSACTIONS OF CHINA ELECTROTECHNICAL SOCIETY 2013 三电参数对铝合金微弧氧化陶瓷膜封孔的影 响 1 2 2 2 李世杰 刘伯颖 李 宾 刘士臣 （1. 河北工业大学材料学院 天津 300129 2. 河北工业大学教务处 天津 300401 ） 摘要 采用不同的电参数，对铝合金微弧氧化陶瓷膜在硝酸铝溶液中进行封孔处理，研究脉 冲模式、电压、频率、封孔时间、占空比对封孔效果的影响。通过大量实验研究发现，在双向脉 冲模式下，最佳封孔工艺参数为：频率200Hz ，占空比均为40% ，封孔电压70～90V ，封孔时间 30～45min 。测试了封孔前后陶瓷膜在质量分数为 5% 的 NaCl （pH=7 ）溶液中的极化曲线，结果 表明经双脉冲封孔处理后，陶瓷膜的耐腐蚀性能得到了显著提高。 关键词：微弧氧化 陶瓷膜 脉冲电源 封孔 中图分类号：TM21 Effect of Electric Parameters on Hole Sealing of Micro-Arc Oxided Ceramic Coatings Formed on Aluminum Alloy Li Shiejie 1 Liu Boying 2 Li Bin 2 Liu Shichen 2 （1. Materials Science and Engineering, Hebei University of Technology Tianjin 300130 China 2. Educational administration, Hebei University of Technology Tianjin 300401 China ） Abstract Using different electric parameters, the micro -arc oxided ceramic membrane formed on aluminum alloy, sealing the holes in aluminum nitrate solution. The research study the effects of hole sealing in different pulse modes, voltages, pulse frequencies, hole seal ing times and duty cycles. A large number of experimental studies show th at, in double pulse mode, the best hole sealing technology parameters are: frequency was 200Hz, duty cycle was 40%, closed voltage was 70V to 90V, closed time was 30min to 45min. The dynamic potential polarization curves of 5% NaCl (pH=7) shows that, double pulse hole sealing can increase the corrosion resistant of ceramic membrane. Keywords ：Micro-arc oxidation, ceramic coating, pulse power, hole sea