卤水氨法纳米氢氧化镁的制备研究.PDF

20 10 1 27 1 Jan. 20 10 CHEM ICAL INDU STRY AND ENG INEER ING V o l. 27 N o. 1 : 1004 - 9533 20 10) 01- 0034 - 04 郑 军, 陈克文, 孙国新 , 257061) : 在常压下氨法合成纳米氢氧化镁方法的基础上, 通过试验, 研究了氨水 pH 值M g2+ 浓度氨 水滴 速度温度和分散剂用量等因素对纳米氢氧化镁制备的影响根据 XRD 和 SEM 测试结果, 提出了制备纳米氢氧化镁的适宜工艺条件: 氨水的 pH 值 135氯化镁溶液浓度为 05 m ol/L氨水 的 料速度 20 mL /m in反应温度 50~ 60 反应时间 60 m in分散剂用量为M gC l 量的 2% 和理 2 想溶剂为乙醇和水的混合溶剂, 其体积比为 1 2~ 1 1 : 卤水; 氨水; 纳米氢氧化镁 : TQ 1322 : A Preparation of N anom eterM agnesium H ydroxide w ith Brine and Amm onia ZH ENG Jun, CHEN Kew en, SUN Guox in Shandong Sh ida Shenghu a Ch em ical L td. , D ongy ing 25706 1, Ch in a) Abstract: N anom eter m agnesium hydrox ide w as prepared by amm onia m ethod under the atm ospheric pres sure. The in fluences of pH o f amm onia, concentrat ion o fM gC l , rate o f amm onia addtion, reaction tem 2 perature and d ispersant dosage w ere stud ied. B ased on the test results o f XRD and SEM, the optmi a l techno log ica l cond itions for nanom eterm agnesium hydrox ide are as follow s: the pH o f amm onia is 14; the concentration of M gC l is 05 m o l/L; the rate of add ing amm onia is 20 mL /m in; the reaction tem pera 2 ture is 50 ! 60 and the tmi e is 60 m in; the d ispersant dosage is 2% w e ight ofM gC l; the idea l so l 2 vent