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View Article Online / Journal Homepage / Table of Contents for this issue
JOURNAL O F ANALYTICAL ATOMIC SPECTROMETRY, DECEMBER 1994,VOL. 9 1389
Analysis of Platinum Powder by Glow Discharge Mass Spectrometry
Mark van Straaten, Karin Swenters and Renaat Gijbels*
Department of Chemistry, University of Antwerp (UIA), Universiteitsplein 1, 8-2610 Wilrijk-Antwerp, Belgium
Jozef Verlindent and EddyAdriaenssens
Union Miniere,A. Greinerstraat 14,B-2660 Hoboken, Belgium
.
M
A
A study was carried out to evaluate the applicability of glow discharge mass spectrometry (GDMS) for the
7
4
: direct analysis of platinum powder. The relative sensitivity factors (RSF)for the different elements of interest
4
2 were determined by the analysis of Pt samples doped with impurities of several elements in a broad
:
2
8 concentration range. These RSFs were used to quantify the results obtained for the analysis of a well
1
0 characterized Pt powder. The investigation illustrated that an accuracy of about 10-15% and a repeatability
2
/
9 of !%lo% are achievable with GDMS for this sample type. The analytical figures of merit of GDMS were
1
/
9 compared with those of other spectrometric techniques normally applied for the determination of platinum.
n
o The simple sample preparation, sensitivity and speed of analysis were found to be valuable assets of GDMS.
S
A Keywords: Glow discharge mass spectrometry; platinum powder analysis; elemental mass spectrometr
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