土壤植物样品中多环芳烃PAHs分析方法研究-应用生态学报.pdf

土壤植物样品中多环芳烃PAHs分析方法研究-应用生态学报.pdf

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1995 1 6 1 CHINESE JOURNAL OF APPLIED ECOLOGY,Jan. 1995, 6( 1) 9296 ( PAHs) * 宋玉芳 区自清 孙铁珩 ( , 110015) A Yediler G Lorinci A Kettrup. , . , .  ( ) . , , (HPLC) , . , PAH 45. 68 93.4277.59 108. 13 79. 11 98.96% . , ; . , . ( ) . Analytical method of polycyclic aromatic hydrocarbons PAHs in soil and plant samples Song Yufang, Ou Ziqing and Sun Tieheng (Institute of App lied Ecology, Academia Sini ca, Shenyang 110015) , A. Yediler, G. Lorinci and A. Kettrup ( Forschungszentrumf r Umwelt und Gesundheil GmbH Institute of Ecological Chemistry N urherberg Germany, , , 85758) . Chin.J. App l.Ecol. , 1995, 6( 1) : 92 96. Soil, plant and seed samples are respect ively extracted by tetrahydrafuran, methanol and ethyl acetate ult rasonically. T he extracts are evaporated by rot ary evaporator, cleaned up on silica gel column and analysed on HPLC w ith fluorescence detector T he recovery of. PAHs is 45. 68 93. 42% for soil, 77. 59 108. 13% for plant, and 79. 11 98. 96% for seed, depending on the physico chemical properties of individual PAH compounds. Dichloromet hane and t etrahydrafuran are t he suitable ext racting agents for soil, and methanol and et hyl acet ate for plant and seed respectively This method has the charac, . teristics of simplicity, rapidity, sensitivity and reliance, and can be used for the study of PAHs in soil plant system. Key wordsHPLC, Soil and plant analysis, Polycyclic aromatic hydrocarbons. [ 1, 4] , , 1 , EPA . , . [ 2, 6, 7] . 2 [ 1, 3, 8, 9] . 60 2. 1 , . , 2. 1. 1 ( ,

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