markes热脱附培训教材.doc

Markes???(TD) ?????? Agilent?????? ?キ ? ???????800 820 3278 ???????800 820 1182 ????Ё????021????Ё????021????Ё??キ? Rev. 1.0 Page 1 of 20 ? ? ?????乍?3 ??Unity ????? 4 ??Unity ??????????? 6 1ˊSet Gas Flows 6 2ˊHeat Trap 7 3ˊExchange Split Tube 8 4ˊShow Carrier Schematic 9 5ˊLoad Method/Sequence 9 6ˊCheck for Leaks 9 7ˊReset Ultra 11 ??Method ??? 12 ??Sequence ??? 14 ??Sequence ??? 17 ??????????? 18 Rev. 1.0 Page 2 of 20 ?????乍? 1ˊ??????乏??99.9995%???????TD????????????? ?????????????TD???????GC?GC/MS?催? 2. 偅???????Cold Trap???????ぎ???????Dew Point??乏 ?ˉ35???????Cold Trap???????????????50psi? 3. Leak Test????????????Unload??Sample Tube??Tray?????? ????Close???に?? 4ˊ???Sample Tube Load???Ё??Sequence? 5ˊ????????????Sample Tube?Cold Trap???????????? ???Tube??偀????????ぎ?????? 6ˊ????????????????????Split Tube? 7ˊ??Sample Tube?Cold Trap???????к?????????????? ????????Tube?Cold Trap???????????????ㄝ? 8ˊ?GC?Inlet????????????Splitless?Purge Flow to Split Vent??? ??999.99min????? Rev. 1.0 Page 3 of 20 ? ?Unity ????? ??????Unity?????Start Program Unity??Unity??? ?????“Detecting Unity Please Wait”?????????? Unity ???? ??? Downloading Firmware ????????????????? ????“Select Options”???????偸???????????????? ??偸????????????⑤????????????????????⑤? ????“Cycle power and retry”?????? Unity?????????Firmware????????????偸?????? Rev. 1.0 Page 4 of 20 ???????????⑤???????Unity??П???????????? ?????Unity????????????downloading Firmware??????? ??咘????Firmware??Download???????????????downloading Firmware??Ё???????????? Firmware Download???????????????? Rev. 1.0 Page 5 of 20 ? ?Unity ??????????? 1ˊSet Gas Flows ??????Desorb Flow????????Set Gas Flows??? ????????????????OK????????????????? ??????“NO”?????????????? ??????NV3?????????50mL/min??????????? ? ?????????GC????????Inlet?Total Flow???? ????????????????Desorb Flow?GC??????????? ???????????????GC???Ё??????????????Desorb Flow?50mL/min??Split????? Unity?Standby?????Ё????Ё?Split On???SV2????????