氯雷他定原料检验-Stabilwax-3.0.pdfVIP

® Pro EZGC Chromatogram Modeler Untitled. Click here to edit. 4 6 8 10 12 14 16 Column: MEGA-WAXPLUS, 60.00 m, 0.32 mm ID, 1.00 µm Carrier Gas: Nitrogen, Constant Flow @ 3.00 mL/min Average Velocity: 37.57 cm/sec Outlet Pressure 101.33 kPa (Atmospheric Pressure) (abs): Oven Temp: 35 °C (hold 10 min) to 200 °C @ 20 °C/min (hold 3 min) Peaks tR R Peak T S peak (min) Width (°C) (min) 1. n-Hexane 3.25 155 0.023 40.0 2. Acetone 6.86 26.1 0.076 40.0 3. Tetrahydrofuran 8.85 26.1 0.104 40.0 4. Isopropanol 11.78 2.5 0.063 75.6 5. Methylene Chloride 11.94 2.5 0.061 78.7 6. Acetonitrile 13.77 5.1 0.044 115.4 7. Chloroform 13.99 5.1 0.041 119.9 8. Toluene 14.45 11.1 0.041 128.9