2468樟脑由newp0rt1于2011年11月22日星期二.pdfVIP

2468 Calcium / Official Monographs USP 35 Limit of free undecylenic acid—Transfer 10 g of Calcium duced in a blank test with the same quantities of the same Undecylenate, accurately weighed, to a 400-mL beaker, add reagents and 0.050 mL of 0.020 N hydrochloric acid (0.035%). 250 mL of solvent hexane, and mix for 2 hours using a mag- netic stirrer. Filter into a 500-mL flask, evaporate with the aid of a current of air to about