ASTM D2077-92 美国材料与试验协会标准.pdfVIP

Designation:D2077–92(Reapproved1998)

StandardTestMethodfor

AshinFattyQuaternaryAmmoniumChlorides1

ThisstandardisissuedunderthefixeddesignationD2077;thenumberimmediatelyfollowingthedesignationindicatestheyearof

originaladoptionor,inthecaseofrevision,theyearoflastrevision.Anumberinparenthesesindicatestheyearoflastreapproval.A

superscriptepsilon()indicatesaneditorialchangesincethelastrevisionorreapproval.

ThistestmethodwaspreparedjointlybyASTMandtheAmericanOilChemists’Society.

1.Scopecrucibleuntilthespecimenignites.Reducethesizeofthe

1.1Thistestmethodcoversthedeterminationofthenon-flameuntiltheheatisjustsufficienttokeepthespecimen

volatilematterremainingafteraspecimenoffattyquaternaryburning.Continuetheheatingofthespecimentoablackchar

ammoniumchlorideiscompletelyburnedandignited.andtransferthecrucibletothemufflefurnace,heatat550to

1.2Thisstandarddoesnotpurporttoaddressallofthe600°Cfor1h.Removethecruciblefromthefurnace,cool

safetyconcerns,ifany,associatedwithitsuse.Itistheslightly,placeinadesiccator,andcooltoroomtemperature.

responsibilityoftheuserofthisstandardtoestablishappro-Weighandrepeattheheatinginthemufflefurnacetoconstant

priatesafetyandhealthpracticesanddeterminetheapplica-weight.

bilityofregulatorylimitationspriortouse.4.Calculation

2.Apparatus