Na_(2)SiO_(3)浓度对铝锂合金微弧氧化膜组织与性能的影响.pdfVIP

HotWorkingTechnology2023,Vol.52,No.4

NazSiO3浓度对铝锂合金微弧氧化膜

组织与性能的影响

刘停，刘春忠，卢天倪，张洪亮，朱明伟，王继杰

(沈阳航空航天大学材料科学与工程学院，辽宁沈阳110136)

摘要：采用微弧氧化法在铸态AI-Li合金表面制备氧化膜层。通过SEM、XRD、显微硬度测试和摩擦摩损测试等

方法分析NazSiO浓度(0.05、0.07、0.09mol/L)对铝锂合金微弧氧化膜组织与性能的影响。结果表明：氧化膜层分为靠近

基体的致密层和外部疏松层两层，主要由α-Al,O，相和-Al,O，相组成。随着硅酸钠浓度的增加，膜层中微孔的数量变

多，膜层厚度及Al.O，的含量均呈现出先升高后降低的趋势。当硅酸钠浓度为0.07molL时，膜层硬度为1171HV,摩擦

系数为0.49,此时膜层耐磨性最佳。

关键词：铝锂合金；NazSiO，浓度；微弧氧化；耐磨性

D0I:10.14158/ki.1001-3814

中图分类号：TG174.453文献标识码：A文章编号：1001-3814(2023)04-0090-05

EffectofNa,SiO,ConcentrationonMicrostructureandProperties

ofMicro-arcOxidationFilmonAl-LiAlloy

LIUTing,LIUChunzhong,LUTianni,ZHANGHongliang,ZHUMingwei,WANGJijie

(SchoolofMaterialsScienceandEngineering,ShenyangAerospaceUniversity,Shenyang110136,China)

Abstract:Theoxidationfilmwaspreparedonthesurfaceofas-castAl-Lialloybymicro-arcoxidation.Theeffectsof

Na,SiO;concentration(0.05mol/L,0.07mol/L,0.09mol/L)onthemicrostructureandpropertiesofmicro-arcoxidationfilm

onAl-Lialloywereanalyzedbyscanningelectronmicroscope(SEM),X-raydiffractometer(XRD),microhardnesstestand

frictiontest.Theresultsshowthattheoxidationfilmsarecomposedofdenselayernearthesubstrateandouterlooselayer,

whicharemainlycomposedofα-Al,O;phaseand-AlO,phase.Withtheincreaseofsodiumsilicateconcentration,the

numberofmicroporesonthefilmincreases,andthefilmthicknessandAl,O;contentincreaseatfirstandthendecrease.When

theconcentrationofsodiumsilicateis0.07mol/L,thehardnessandcoefficientofthefilmare1171HVand0.49,respectively,

andthewearresistanceofthefilmisbest.

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