45万吨年甲醇精馏工段及加压塔第二冷却器设计.docVIP

摘 要 本文对双塔流程、三塔流程和四塔流程工艺进行了阐述,显示了四塔流程的优越性。对甲醇精馏工段全流程进行物料衡算,着重预精馏塔的工艺设计。应用ASPEN PLUS化工模拟系统中的和DSTUW、RADFRAC塔精馏模块对预精馏塔进行模拟。通过本课题的设计了解甲醇精馏的发展历程和国内外的研究现状，熟悉甲醇精馏工艺流程、技术设备等。通过对甲醇精馏工艺流程的物料衡算和能量衡算及换热器的设计与选型掌握甲醇精馏工业生产中各塔的作用、进出料情况、塔板数等相关参数的计算。最后绘制出工艺流程图、带控制点的物料流程图、设备图和设备布置图。 关键词:甲醇精馏 ;预精馏塔;工艺设计;Aspen Plus;流程模拟 Abstract this paper employed two columns rectification process,three columns rectification process and four columns rectification process were discussed in methanol rectification technology ,showed the advantage of the four columns rectification process.Calculate the work section of methanol distillation mass balance,pressed on the process planning of the fore distillation tower .The fore distillation tower of methanol were simulated by using the RADFRAC、DSTUW rectification modules of ASPEN PLUS chemical industry simulation system .Understanding of this issue through the design development process and the methanol distillation research status at home and abroad, familiar with the methanol distillation process, and technical equipment. Methanol distillation process through the material balance and energy balance and heat exchanger design and selection of control in the industrial production of methanol distillation tower role, access to material conditions, plate number and other relevant parameters of the calculation. Finally draw the process flow chart, flow chart with a control point of materials, equipment layout drawings and equipment. Keywords: Methanol Distillation ; fore distillation tower; process planning ; Aspen Plus;Process Simulation 目录 摘 要 I 前言 1 第一章 综述 2 1.1概述 2 1.1.1甲醇的性质及用途 2 1.1.2 甲醇的用途 2 1.1.3 甲醇在新技术中的应用 3 1.1.4 粗甲醇的组成 4 1.2工艺流程选择 5 1.2.1普通双塔流程 5 1.2.2高质量三塔精馏工艺[4] 7 1.2.3节能型三塔流程[5] 8 1.3选择甲醇工艺流程的依据[7] 12 1.4国内外甲醇生产的概况 12 1.4.1 国内外甲醇工业现状 12 1.4.2 国内外甲醇生产工艺技术 13 1.5甲醇精馏残液回收技术 18 1.5.1甲醇污水处理技术的发展状况 18 1.5.2甲醇污水处理工艺 18 1.6换热器 19 1.6.1换热器分类 19 1.6.2管壳式换热器工艺设计 20 第二章 四塔流程工艺条件的设计 24 2.1物料衡算 24 2.1.1操作条件 24 2.1.2物料衡算 24 2.2 ASPEN PLUS工艺流程模拟 30 2.2.1四塔的简