重氮化反应 氨基变烃基 1-(p-NITROPHENYL)-1,3-BUTADIEN.pdfVIP

Organic Syntheses, Coll. Vol. 4, p.727 (1963); Vol. 31, p.80 (1951). p 1-( -NITROPHENYL)-1,3-BUTADIENE p [1,3-Butadiene, 1-( -nitrophenyl)-] Submitted by Gus A. Ropp and Eugene C. Coyner1. Checked by Arthur C. Cope and David J. Marshall. 1. Procedure A. 1-(p-Nitrophenyl)-4-chloro-2-butene. p -Nitroaniline hydrochloride is prepared by heating 138 g. (1.0