干燥失重和硫酸盐灰分-附录EP.docVIP

Ph. Eur. method 2.2.32) Loss on drying is the loss of weight expressed as % w/w. Method Place the prescribed quantity of the substance to be examined in a weighing bottle previously dried under the conditions prescribed for the substance to be examined. Dry the substance to constant mass or for the prescribed time by one of the following procedures. Where the drying temperature is indicated by a single value rather than a range, drying is carried out at the prescribed temperature ± 2 °C. a) in a desiccator: the drying is carried out over diphosphorus pentoxide R at atmospheric pressure and at room temperature; b) in vacuo: the drying is carried out over diphosphorus pentoxide R, at a pressure of 1.5 kPa to 2.5 kPa at room temperature; c) in vacuo within a specified temperature range: the drying is carried out over diphosphorus pentoxide R, at a pressure of 1.5 kPa to 2.5 kPa within the temperature range prescribed in the monograph; d) in an oven within a specified temperature range: the drying is carried out in an oven within the temperature range prescribed in the monograph; e) under high vacuum: the drying is carried out over diphosphorus pentoxide R at a pressure not exceeding 0.1 kPa, at the temperature prescribed in the monograph. If other conditions are prescribed, the procedure to be used is described in full in the monograph. 取规定量的样品置已干燥的称量瓶中，干燥称量瓶的条件与样品一致。在下述条件之一中，干燥样品至恒重或至规定的时间。当规定的干燥温度是单一值而不是范围时，干燥时温度为规定值± 2 °C a)“干燥器中”：室温常压下干燥，干燥剂为五氧化二磷。 b) “真空”：室温，压力为1.5 kPa ～ 2.5 kPa下干燥 ，干燥剂为五氧化二磷。 c) “规定温度下真空”：温度为规定值，压力为1.5 kPa ～ 2.5 kPa下干燥 ，干燥剂为五氧化二磷。 d) “在烘箱中，指定温度范围”：在烘箱中，指定温度范围下干燥 e) “高真空”：温度为规定值，压力不超过0.1 kPa下干燥，干燥剂为五氧化二磷干燥。 如专论中另有说明，按专论中所述操作。Appendix IX A. Determination of Sulphated Ash 附录IX A硫酸盐灰分： （除非另有说明，使用方法1） Method I Heat a platinum dish to redness for 10 minutes, allow to cool in a desiccator and weigh. Unless otherwise specified in the monograph, place 1 g of the substance being examined in the