Ce+掺杂纳米+SnO2粉体的制备及其结构表征.pdfVIP

Journal of Xi an Polytechnic University Vol No Sum No X DOI issn x j C e S n O SnO Ce SnO X XRD TEM X XPS Ce SnO Ce Ce SnO SnO Ce SnO T Q A Preparation and nanostructure characterization of Cedoped SnO nanopowders H OU Jinli QIU Runhong X UE Y uany uan FU Chong Teaching Affairs Department Xian Polytechnic University Xian China School of Mechanical and Electrical Engineering Xian Polytechnic University Xian China Abstract In order to improve the high temperature stability of the SnO nanopowders a series of Cedoped SnO nanopow ders with various doping concentrations were prepared by chemical co recipitation technique and the prepared nanopow ders were characterized by X ray diffrac p tion XRD transmission electron microscopy TEM and Xray photoelectron spectroscopy XPS The results show that Ce doping can obviously prevent the grow th of nanosized SnO crystallites When the molar ratio of Ce reaches and surpasses SnO crystallite size rea ches a minimum value and remains almost constant The effect of Ce doping on hindering crys tallite grow th can be attributed to the solute drag and lattice distortion resulting from Ce dis solving in the bulk phase of SnO to form solid solution BS Email houjinli com Ce SnO Key words