Fe2O3@SrTiO3纳米复合材料的制备与光催化性能研究.pdf

FezO。@SrTiO。纳米复合材料的制备与光催化性能研究／李晓敏等 · 37· Fe203@SrTi03纳米复合材料的制备与光催化性能研究’ 李晓敏，王光辉，徐乾，安 良，高 芳，陈文靖 (武汉科技大学化学工程与技术学院，武汉430081) 摘要 采用溶剂热法制成纳米纺锤体Fe203，再采用溶胶一凝胶法制成Fe2G@SrTiQ纳米复合材料，并对其 进行SEM、IR、EDS、XRD表征。SEM显示制备了纳米纺锤体Fe203和Fe2 03为赤铁矿晶型，掺杂的SrTi03为无定形态。针对偶氮类染料橙Ⅱ的 都证明Sr，ri03负载成功；XRD表征显示Fe2 光催化实验表明，复合材料的光催化性能优于纯Fe203和纯srTiQ，且随着SrTiOs含量的增加，光催化活性增强。 当SrTiQ制备过程中所加前驱体剂量为17．0 g时，橙Ⅱ的去除效率为37．5％。 关键词 Fe20s@SrTiOs纳米复合材料光催化 中圈分类号：TB331；0633 文献标识码：A and ofFe203@SrTi03 PreparationPhotocatalyticProperties LI Xiaomin，WANG Qian，ANLiang，GAOFang，CHENWenjing Guanghui，XU ofChemical and ofScienceand 430081) University Technology，Wuhan (College EngineeringTechnology，Wuhan Nano was solvothermalmethod．Then nanocom— Abstract Fe203 synthesized Fez03@SrTi03 spindle through werecharacterized and were method．The SEM，EDX，IR posites synthesizedthroughsol-gel as-preparedsamples by diffraction．TheSEM of indicatedthatthe hadbeen FezOs Fe203@SrTi03nanoeomposite X-ray imagesnano-spindle was ininfraredandEDX that nanostructurewascoatedonthesur— found srTi03 synthesizedsuccessfully．It spectra that faceofthe ofthe showedthestructureofFez03wasahematite nano-spindle№03．Ⅺmpatternssamples crys—