黄芩中黄芩苷的分离与结构表征.pdfVIP

2007 11 中成 药 Novem ber 2007 29 11 Ch ine e T rad itional P aten tM ed icine V o.l 29 No. 11 2 1 1 1 2 李云霞 , 索全伶 , 贺文智, 李春萍, 黄延春 ( 1. 内蒙古工业大学化工学院, 内蒙古 呼和浩特 01005 1; 2. 内蒙古师范大学化学与环境 学学院, 内蒙古 呼 和浩特 010022) : ; ; ; : : , : , , ( FT IR )-( UV-V i ) 1 13 ( M S)( H-NM R) ( C-NM R): 60 g 3. 17 g, 5. 29% ; 1. 55 g 0. 36 g, 23. 2% , : 5, 6- 7-O--D- (), C H O 21 18 11 : R284. 1 : A : 1001-1528( 2007) 11-1648-03 Separation and structural characterization of baicalin in S cutellar ia ba ica lensis G eorgi 2 1 1 1 2 LI Yun-x ia , SUO Quan-ling , HE W en-zh i, LI Chun-ping , HUANG Y an-chun (1. College of Chem icalE ng ineering, InnerM ongolia P olytechnic University, H ohho,t 010051, Ch ina; 2. College of Chem ical an Env ironm ental Sci- ence, InnerM ong oliaN ormal University, H ohhot, 010022, China) KEY W ORD S: Scutellaria baicalensis Georg;i baicalin; eparation; tructural character ization ABSTRACT A IM: Active com ponent w a eparated from Scutellaria baicalensis Georg i and it com po ition and m olecu lar tructurew ere characterized. METHOD S: The crude productw a eparated from S cutellaria baicalensis by alcohol extraction and acid precipitation. U ing reiterant recry tallization m ethod, yellow need le cry tal w a 1 13 gained. The com po ition and m olecular tructure w ere characterized by FT IR, UV-V i, MS and H-, C-NMR. RE SULTS: 3. 17 g yellow pow der w a eparated from 60 g Scutellaria baicalensis and 0. 36 g cry talw a gained