《Effect of sintering atmosphere on composition and properties of NiFe2O4 ceramic》.pdfVIP

《Effect of sintering atmosphere on composition and properties of NiFe2O4 ceramic》.pdf

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J. Cent. South Univ. (2015) 22: 450−454 DOI: 10.1007/s11771-015-2542-6 Effect of sintering atmosphere on composition and properties of NiFe O ceramic 2 4 TIAN Zhong-liang( 田忠良), ZHANG Teng(张腾), LIU Kai(刘恺), LAI Yan-qing(赖延清), LI Jie(李劼) School of Metallurgy and Environment, Central South University, Changsha 410008, China © Central South University Press and Springer-Verlag Berlin Heidelberg 2015 Abstract: NiFe O ceramics were prepared in different sintering atmospheres. The phase compositions, microstructures and 2 4 mechanical properties were studied. The results show that the stoichiometric compound NiFe O cannot be obtained in vacuum or 2 4 atmospheres with oxygen contents of 2×10−5, 2×10−4 and 2×10−3, respectively. All the samples sintered in above-mentioned atmospheres contain phases of NiFe O and NiO. With increasing oxygen content, NiFe O content in the ceramic increases, while 2 4 2 4 NiO content appears a contrary trend. In vacuum, NiFe O ceramic has average grain size of 3.94 μm, and bending strength of 2 4 85.12 MPa. The changes of the phase composition and mechanical properties of NiFe O based cermets are mainly caused by the 2 4 alteration of their properties of NiFe O ceramic. 2 4

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