200andmoreNMRexperimentsapracticalcourse.docVIP

200 and More NMR Experiments : A Practical Courseby Stefan Berger, Siegmar Braun ReviewThis book is an excellent catalogue of useful NMR experiments for people who are looking for the most suitable experiment to solve a specific problem.It collects in one place all the currently pulse sequences from liquid NMR spectroscopy, discusses their relative merits, the time required to perform them and gives experimental examples measured by the authors for this book. ... In conclusion, I think this book is a great encyclopedia of the techniques of modern liquid state NMR spectroscopy. It is highly readabele and should be on the shelf of any serious NMR spectroscopist, who does more complicated experiments than routine H-NMR spectroscopy. Finally instrument vendors should consider packing at least one copy of this book with every new NMR machine and using it as an educational toot when installing the machine. Book DescriptionThis work-book will guide you safely, in step-by-step descriptions, through every detail of the NMR experiments within, beginning with 1D routine experiments and ending with a series of advanced 3D experiments on a protein:· Which experiment can best yield the desired information?· How must the chosen experiment be performed?· How does one read the required information from the spectrum?· How does this particular pulse sequence work?· Which other experiments give similar information?This third edition of the book, following its two highly successful predecessors, has been revised and expanded to 206 experiments. They are organized in 15 chapters, covering test procedures and routine spectra, variable temperature measurements, the use of auxiliary reagents, 1D multipulse experiments, spectra of heteronuclides, and the application of selective pulses. The second and third dimensions are introduced using pulsed field gradients, and experiments on solid state materials are described. A key part describes 3D experiments on the protein ubiquitin wi