南极磷虾产品关键质量指标检测方法地研究.pdf

Abstract AntarctickrillISthe of inAntarcticPole．It1Snot keyspecmsecosystem only alsorichinnutritionalvalue．Ithasthecharacteristicsof resources，but huge high andSOon．Inrecent tothe protein，lowlipid years，Ourcountrygraduallyenlarges researchand ofAntarctickrill．The modeofAntarctickrillof development processing our fromtheinitial to country machiningdeep graduallydevelop processing，rough the andutilizationofAntarctic achieve processingdirection．Ultimatelydevelopment krill products． 1、HPLCmethodfordeterminationofastaxanthinisomersinAntarctickrilloil wasestablishedafter a having bysolid-phase pre-separation researchonthe additionofNaOH— experimental by pre-separation，saponification YMC·Carotenoidthreeastaxanthinisomerswere methanol，separationby C30，the obtained。Then externalstandardmethod．The quantifiedby optimumpurification conditionsforastaxanthininAntarctickrilloilwereasfollows：Withassolid LC．NH2 extraction elution phase column，hexane—acetone—methanol(1：2：2)as agents，elution volumeat8mL，flow at2-4 mL／min．After solid velocity L