04 The application of EQCM to the study of the electrochemical behavior of propylene carbonate solutions文献.pdfVIP
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JOUANAL OF
ELSEVIER Journal of Electroanalytical Chemistry 393 (1995) 43-53
The application of EQCM to the study of the electrochemical behavior
of propylene carbonate solutions
D. Aurbach *, A. Zaban
Department of Chemistry,Bar-llan University,Ramat Gan 52900,Israel
Received 18 January 1995; in revised form 9 March 1995
Abstract
The electrochemical behavior of gold electrodes in propylene carbonate (PC) solutions was investigated using an electrochemical
quartz crystal microbalance (EQCM). The solutions studied included uncontaminated LiAsF6 and LiPF6 solutions, and CO2 and
H20-containing LiAsF6 solutions. Surface film formation on the electrodes in these solutions was investigated during a potential scan
from the open-circuit potential (OCV) to 0.5 V vs. Li/Li + and during potential steps from the OCV to various lower potentials. The data
obtained from the EQCM experiments were analyzed with the help of the results of previous spectroelectrochemical studies of several
surface species formed on noble metal electrodes in these solutions. Analysis of the EQCM data enabled the definition of potential
domains in which salt anion, solvent or contaminant reduction are dominant. Using this technique it was also possible to follow the
dissolution processes of surface species and hydration of hygroscopic surface film compounds in water-contaminated solutions. The
results obtained
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