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分子筛分离乙醇和水.pdf

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分子筛分离乙醇和水

0263–8762/04/$30.00+0.00 # 2004 Institution of Chemical Engineers =titleshtm Trans IChemE, Part A, July 2004 Chemical Engineering Research and Design, 82(A7): 855–864 SEPARATION OF ETHANOL–WATER MIXTURES USING MOLECULAR SIEVES AND BIOBASED ADSORBENTS S. AL-ASHEH*,{, F. BANAT and N. AL-LAGTAH Department of Chemical Engineering, Jordan University of Science and Technology, Irbid, Jordan he potential use of new biobased adsorbents and different types of molecular sieve was T assessed in the separation of the ethanol–water azeotrope. Molecular sieves of type 3A, type 4A, and type 5A and biobased adsorbents such as natural corncobs, natural and activated palm stone and oak, were used in this study. Each of these adsorbents was packed in a column, which was surrounded by a heating jacket. The jacket temperature was maintained constant in an attempt to maintain the packed-column at constant temperature. The water concentration in the feed solution was varied from 5% to 12% (weight basis). Although the initial concentration of ethanol in the ﬂask was constant at the beginning of the experiment, it varied with time due to boiling. The breakthrough curves of water sorption on these adsorbents at different water contents showed that among the molecular sieves examined, type 3A