美国瓦里安4000GC-MS使用维护和常见故障排除技术总结.pptVIP

* * * * Packed injector inserts provide strong advantages for some analyses and shown here. Either fused silica or borosilicate glass wool can be used for most applications but fused silica is more inert for active compounds such as phenols. Use glass wool sparingly because too much wool increases the active compound adsorption. A one-centimeter plug of loosely bound wool is sufficient for most applications. * * The choice of solvents for a a chromatographic analysis depends on the component solubility, the detector, and the polarity of the analytical column. Ideally, solvents should match the polarity of the column, especially when injecting large volumes and performing on-column or splitless injections. Non-polar columns perform best with non-polar solvents. Polar columns perform best with polar solvents, however, they also perform well with non-polar solvents. These are the recommended solvents for non-polar columns... * * And here are suggested solvents for Intermediate and Polar columns. * * Now that we have addressed the front end of the GC/Mass Spectrometer we will look at some initial checks to verify the detector condition. * * Before using the mass spectrometer to acquire GC/MS data, there are some key checks that need to be performed. These checks will be performed in one three different sections of Saturn System Control. * * In the Diagnostics dialog we can quickly check overall ion trap functionality. Diagnostics tests should be performed after column replacement or Ion Trap Cleaning. Observe the different reporting areas on the diagnostics display, including results of checks on temperature zones and ionization system voltages. Performance of the Vacuum System can be checked by observing Turbo Pump Speed and the operating Current. Changes in these parameters can alert you to a possible leak or bearing wear. The Ion Gauge, if installed, will display the working pressure in the Ion Trap * * In the Diagnostics dialog we can quickly check overall io