Lab G1 Preparing a solution from a solid.docVIP

Lab G1 Preparing a solution from a solid ?What technological skills and procedures are needed to prepare 100.0mL of a 0.100mol/L solution of potassium hydrogen phthalate? ? Procedure: Calculate the mass of the KHC8H4O4(s) needed to prepare 100.00mL of a 0.100mol/L solution. Calculation of the mass of KHC8H4O4(s): n(KHC8H4O4(s))= cv = 0.100mol/L?00.0mL = 10mmol m4(KHC8H4O4(s))= M(KHC8H4O4(s))?0mmol= 2042.3mg =2.05g Measure the calculated mass of KHC8H4O4(s) in a clean, dry 150mL breaker. Dissolve the solid in 40mL to 50mL of pure water. Use a stirring rod to help dissolve the solid. Be sure to rinse the stirring rod over your beaker of solution. Transfer the solution into a 100mL volumetric flask. Rinse the breaker two three times with small quantities of pure water, transferring the rinsing into the volumetric flask. Add pure water to the volumetric flask until the volume is 100.00mL. Use the dropper and meniscus finder for the final few milliliters to set the bottom of the meniscus on the calibration line. Stopper the flask and mix the contents thoroughly by repeatedly inverting the flask. Store the solution for the next lab. Lab G2 Standardizing a Solution by Titration ? Problem: What is the molar concentration of a given sodium hydroxide solution? ?Evidence: Titration of 10.00ml of KHC8H4O4(aq) with Diluted NaOH(aq). Trial 1 2 3 4 Final burette reading(mL) 16.9 26.3 38.4 23.7 Initial burette reading（mL） 2.6 14.3 26.3 11.5 Volume of NaOH(aq) added(mL) 14.3 12.0 12.1 12.2 Indicator color pink Light pink Light pink Light pink ?Analysis: c(KHC8H4O4(aq))= 0.100mol/L n(KHC8H4O4(aq))= cv= 0.100mol/L×100.0ml = 10mmol NaOH(aq) + KHC8H4O4(aq) → KOH (aq) + NaHC8H4O4(aq) *v=12.1mL v=10.00ml c=? c=0,100mol/L * The volume of NaOH(aq). is an average of trials 2,3 and 4. n(NaOH(aq)) = 10mmol × 1/1 = 10mmol c(NaOH(aq)) = n(NaOH(aq))/ v(NaOH(aq)) =10mmol/ 12.1mL =0.8264mol/L =0.826mol/L *the molar concentration of NAOH(aq) is 0.