CoFe2O4米线的制备与表征.docVIP

摘 要: 利用阳极氧化铝（AAO）模板，运用电化学沉积法，并通过后期的氧化处理，获得了CoFe2O4纳米线。X射线衍射显示，纳米线为无晶粒取向的尖晶石结构。从电子显微镜照片可以看出，沉积得到的CoFe2纳米线很疏松，空气氛下的热处理使之转化为致密的CoFe2O4纳米线。扩孔时间40分钟所得纳米线阵列的矫顽力最大，为1.9 kOe（测量磁场平行于纳米线）。 关键词: AAO模板；CoFe2O4纳米线；矫顽力 Abstract: By electrodeposition method and further oxidization, CoFe2O4 nanowire arrays within anodic aluminum oxide (AAO) templates were obtained. The XRD result proved that the phase structure of the nanowires is cubic spinel-type, and they exhibit no preferred crystallite orientation. The TEM images showed that, the CoFe2 nanowires electrodeposited within the t