無酚法二硬脂基季戊四醇亚磷酸酯的合成工艺研究.docVIP

无酚法二硬脂基季戊四醇亚磷酸酯的合成工艺研究唐蓉萍 侯侠（兰州石化职业技术学院石油化学工程系，兰州 730060）[摘 要]介绍了抗氧剂二硬脂基季戊四醇亚磷酸酯的合成方法，并以季戊四醇、三氯化磷和硬酯醇为原料合成了抗氧剂二硬脂基季戊四醇亚磷酸酯。该方法工艺稳定，成本低，产品收率达94%，所用溶剂和催化剂可回收并循环使用。[关键词] 合成；抗氧剂；二硬脂基季戊四醇亚磷酸酯Synthesis of Antioxidant Dialkypentaerythitoldiphosphite by Non-Phenol ProcessTang Rongping Houxia(LanZhou Petrochemical College of Vocational Technology,LanZhou,730060,China)Abstract:A process for the preparation of dialkylpentaerythritol diphosphites which are not contaminated by the presence of phenol. The process utilizes pentaerythritol, phosphorustrichloride as starting materials to prepeare dichlorope