NOVAInstallTrainingModule.pptxVIP

NOVA e-系列培训教程Automated Surface Area and Pore Size Analyzer 培训指南安装准备安装样品管校准样品制备（脱气）样品分析 数据处理异常吸附等温线原因分析案例分析:对BET结果的影响因素安装准备所需装置Two Stage Inert Gas Regulator(CGA 580)WithGas Cut-Off Valveand1/8” Male threadedSwagelok Fitting安装准备Required Utilities高纯氮气≥ 99.999 %电源220 Volt / 50 Hz安装准备PC Pentium Processor20 MB HD SpaceRS232 or USB PortWindows XP, NT, or2000安装准备Liquid Nitrogen Sourceand Transfer DewarMAIN气路连接Connect Gas line to the two stage gas regulator(7/16” Wrench required for tightening)气路连接Connect the other end of the gas line to the threaded gas connector fitting on the back of the NOVA.(7/16” Wrench required for tightening)真空管路连接Vacuum Hose ConnectionConnect vacuum hose to the back of the NOVAConnect vacuum hose to the vacuum pump通讯电缆连接Communication Cable ConnectionConnect RS232 cableto the 9 Pin connectors on the PC and NOVA.电源线连接Power Line ConnectionPlug power cord into NOVA and into a 110 V AC power sourcePower Up The SystemTurn on vacuum pump.Set gas pressure at 10 psig on regulator and open gas valve.Insert NOVA User disk.Turn on NOVA power switch.软件安装Install NOVAWin From CD建立NOVA-PC通讯Establish NOVA To PC CommunicationOpen NOVAWin program建立NOVA-PC通讯Establish NOVA To PC CommunicationSelect “Operation” menu and click “Instrument Settings”Establish NOVA To PC CommunicationSelect the COM port number that will be used for communicating with the NOVA.Establish NOVA To PC CommunicationSelect “Operation” menu and click “Instrument Status” to verify the PC is communicating with the NOVAEstablish NOVA To PC CommunicationNOVA Status:Stations “Idle”出现上述“空转”信息，则安装完成 ！MAIN样品管校正Cell CalibrationOpen NOVAWin softwareCell CalibrationFill dewar to the internal upper mark with liquid nitrogen将液氮倒至杜瓦瓶内标刻度Place sample cell with filler rod into analysis station to be used for calibration!将样品管连同填充棒装入分析站填充棒的作用:减小死体积, 使吸脱附等温线闭合良好.Cell CalibrationSelect Calibrate Cell from the Operation MenuCell CalibrationSelect station to be used for cell calibrationSelect gasfor calibrationAssign a