组会关于CuO阻抗谱的学习(wc).ppt

关于CuO阻抗谱的学习 演讲人：王冲 Group meeting 实验制备部分：In 80ml deionized water，contain 0.2 g of Cu(Ac)2 ·3H2O and 1.5 ml of 28 wt % ammonia, pH value is 10.5. In a stainless steel autoclave with a Teflon linear heated at 150℃ for 8h. After the autoclave was air-cooled to room temperature, black precipitation and colorless solution were obtained. The resulting precipitation was separated by centrifugation, washed with deionized water and ethanol several times, and dried at 60℃ for 12 h. 样品的形貌和XRD图形 从图片中我们可以看到大概有一微米长20纳米厚，200纳米粗的花瓣状的CuO 片状结构。 作为电极的电化学性能----循环伏安曲线图 图a为前3次循环的循环伏安曲线图。可以观察到在图a的第一次CV曲线中的负极扫描中，可以看到3