超纯铟的制备.doc

超纯铟的制备 高远，朱世明 （广东先导稀材股份有限公司 先进材料研究院，广东清远 511517） 摘要：以电解法生产的(4N5)高纯铟为原料，用真空蒸馏脱镉、铊，氢气气氛中进一步区熔提纯，并对重要技术参数进行了优化制备超高纯铟产品直收率大于72%。 关键词：超纯铟区熔真空蒸馏Preparation of Ultra Pure Indium GAO Yuan, ZHU Shi-ming (Research Department of Advanced Materials, Guangdong First Rare Materials Co. Ltd., Qingyuan 510651, Guangdong, China) Abstract: The electrolytic refined high pure indium (In 99.95%, 4N5) was first vacuum distillation volatilized to remove cadmium, thallium and other volatile elements, and then purified with zone melting process in hydrogen atmosphere. Important technical parameters were optimized. The