PET分析方法.pptVIP

PET分析方法 麦德美 一.Master NS9 concentration analysis 1-1.Reagents ①Potassium Hydroxide 50% ②Blue Victoria Indicator ③Chloroform ④Sodium Tetrakis(4-fluorophenyl)borate dihydrate 1-2.Titration Method Take 2 ml of Master NS9 washing solution to be tested and introduce it in a Becker, Add 25 ml of deionised water and 5 ml of Potassium Hydroxide 50%, Add 5 – 10 drops of Blue Victoria Indicator, Add 5 ml of Chloroform, Titrate with Sodium Tetrakis(4-fluorophenyl) borate dihydrate in strong agitation (magnetic stirrer with steel barrel) until colour, of organic bottom phase, changes from p