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Influence of tube wettability on water contact angle of powders determined by capillary rise.pdf

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Influence of tube wettability on water contact angle of powders determined by capillary rise.pdf

Colloids and Surfaces A: Physicochem. Eng. Aspects 492 (2016) 79–87 Contents lists available at ScienceDirect Colloids and Surfaces A: Physicochemical and Engineering Aspects journal homepage: /locate/colsurfa In?uence of tube wettability on water contact angle of powders determined by capillary rise Abdullah Alghunaim, Bi-min Zhang Newby ? Department of Chemical and Biomolecular Engineering, The University of Akron, Akron, OH 44325-3906, United States highlights ? Water contact angle of powder (?w) was assessed by Washburn capillary rise (WCR). ? Packing tube wettability affected ?w determined by WCR. ? A hydrophobic tube increased ?w of a highly wettable powder. ? The effect of tube wettability on ?w was more dramatic by using a smaller tube. graphical abstract article info Article history: Received 19 August 2015 Received in revised form 5 December 2015 Accepted 12 December 2015 Available online 21 December 2015 Keywords: Capillary rise Washburn’s equation Contact angle Tube surface wettability Powder wettability abstract During a recent literature review, we have noticed that researchers used tubes made of materials having a wide range of wettability, including plastics and metals, to pack powders for wettability determination using the Washburn capillary rise (WCR) method. Most studies applying WCR have focused on the effects of powder properties and their packing methods on the contact angle, while neglecting the role of packing tube. Although the ratio of packed powder surface area to tube surface area is large, we believe that tube wettability could have a signi?cant effect on powder wettability determined using the WCR method. In this paper, we report that when water was penetrating the packed powder inside hydrophobic tubes, the water front along the tube wall was severely pinned, and in some cases, it was completely pinned at the support/packing/tube wall interface until the water had penetrated all the way up the packed powder. Using hydrophobic tubes li