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Large reduction in electrical contact resistance of flexible carbon nanotubesilicone rubber composites by trifluoroacetic acid treatment.pdf

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Large reduction in electrical contact resistance of flexible carbon nanotubesilicone rubber composites by trifluoroacetic acid treatment.pdf

Composites Science and Technology 143 (2017) 98e105 Contents lists available at ScienceDirect Composites Science and Technology journal homepage: /locate/compscitech Large reduction in electrical contact resistance of ?exible carbon nanotube/silicone rubber composites by tri?uoroacetic acid treatment Sang-Eui Lee a, Sang Soo Jee a, Hyokeun Park a, Sung-Hoon Park b, Intaek Han a, *, Soichiro Mizusaki a, * a Materials Research Center, Samsung Advanced Institute of Technology, Samsung Electronics, 130 Samsung-ro, Suwon, 446-712, South Korea b Department of Mechanical Engineering, Soongsil University, 369 Sangdo-ro, Donjak-gu, Seoul, 156-743, South Korea article info Article history: Received 24 May 2016 Received in revised form 2 March 2017 Accepted 4 March 2017 Available online 7 March 2017 Keywords: Electrical contact resistance Carbon nanotube Tri?uoroacetic acid Stretchable composite Flexible composite abstract We report a large reduction in contact resistance between stretchable carbon nanotube/silicone rubber composites and silver electrodes by a chemical surface treatment, accompanied by an enhancement in the electrical conductivity of the composites. The reactive solvent, tri?uoroacetic acid, works for the purpose. In addition, the treatment makes a uniform etching in a micro level with little sacri?ce in surface roughness of the nanocomposites. The electrical conductivity of 1.0 wt% nanotube composite was enhanced approximately two-fold and three-fold by ten- and thirty-second treatment, which was induced by the reduction in the contact resistance to one half of an original value. It is meaningful that our ?nding can be an approach to reduce the nanoparticle loading while keeping electrical conductivity in a high level, which can be crucial for securing ?exibility or stretchability in a viewpoint that the elongation is inversely proportional to the conductive particle loading. ? 2017 Elsevier Ltd. All rights reserved. 1. Introduction Carbon nanotubes (CNT)/ela