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Axial mixing and segregation in a gas-liquid-solid three-phase fluidized bed of solid particles of d.pdf

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Axial mixing and segregation in a gas-liquid-solid three-phase fluidized bed of solid particles of d

Pergamon Chum. a/ En!On,ermq S~wmc. Vol 52, NOS. 21.22. pp 3961 3970. 1997 ( 1997 Elsevier ~ i ence Ltd All rights reserved Printed m Great Britain PII : 50009-2509(97)00239-X o~x~9 2509 97 s170~} , 01)0 Axial mixing and segregation in a gas-liquid-solid three-phase fluidized bed of solid particles of different sizes and densities Toshitatsu Matsumoto, *t Nobuyuki Hidaka,* Yohei Takebayasi* and Shigeharu Morooka ~ * Department of Applied Chemistry and Chemical Engineering, Kagoshima University, 1-21-40 korimoto, Kagoshima 890, Japan; : Department of Materials Physics and Chemistry, Graduate School of Engineering. Kyushu University. Fukuoka 812-81, Japan (Accepted 1 July 1997) Abstract. Sieved silica-alumina particles (diameter = 481 lam; density = 1990 kg/m3), glass beads (diameter = 516 lam; density = 2500 kg/m 3) or mixtures thereof were fluidized in a verti- cal bubble column of 7 cm in diameter and 4.50 m in height. The bed was operated batchwise or continuously with respect to the feed ofsolid particles. Axial changes in gas and solid holdups in the bed were measured by simultaneously sectioning the column with 20 horizontal plates. The measured solid holdup of each component in the column was compared with the analytical results calculated by a one-dimensional sedimentation-dispersion model. Both experimental and calculated results were in satisfactory agreement over the entire column, which consisted of dense and dilute regions, as well as circulating quantities of liquid and solid particles. ( 1997 Elsevier Science Lid Kevwords : Bubble column: three-phase fluidization: mixing; segregation: phase holdup. INTRODI_:CTION Three-phase tluidization is an important technique for bringing gas, liquid and solid particles well into contact and is widely used in petroleum and bio- chemical processes. When mixed solid particles are used as the solid phase, a natural segregation of com- ponents occurs in the bed. Many studies (Smith et a