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Modifying of Cotton Fabric Surface with Nano-ZnO Multilayer.pdf

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Modifying of Cotton Fabric Surface with Nano-ZnO Multilayer

NANO EXPRESS Modifying of Cotton Fabric Surface with Nano-ZnO Multilayer Films by Layer-by-Layer Deposition Method S?ule S. Ug?ur ? Merih Sar??s??k ? A. Hakan Aktas? ? M. C?ig?dem Uc?ar ? Emre Erden Received: 13 April 2010 / Accepted: 30 April 2010 / Published online: 25 May 2010 The Author(s) 2010. This article is published with open access at S Abstract ZnO nanoparticle–based multilayer nanocom- posite films were fabricated on cationized woven cotton fabrics via layer-by-layer molecular self-assembly tech- nique. For cationic surface charge, cotton fabrics were pretreated with 2,3-epoxypropyltrimethylammonium chlo- ride (EP3MAC) by pad-batch method. XPS and SEM were used to examine the deposited nano-ZnO multilayer films on the cotton fabrics. The nano-ZnO films deposited on cotton fabrics exhibited excellent antimicrobial activity against Staphylococcus aureus bacteria. The results also showed that the coated fabrics with nano-ZnO multilayer films enhanced the protection of cotton fabrics from UV radiation. Physical tests (tensile strength of weft and warp yarns, air permeability and whiteness values) were per- formed on the fabrics before and after the treatment with ZnO nanoparticles to evaluate the effect of layer-by-layer (LbL) process on cotton fabrics properties. Keywords Layer-by-layer deposition ZnO nanoparticle Multilayer Antibacterial activity UV protection Introduction Layer-by-layer assembly (LbL), invented by G. Decher, is a unique technique for the fabrication of composite thin films. The sequential adsorption of oppositely charged polycations and polyanions on solid surfaces leads to the buildup of polyelectrolyte multilayer films. The sequential multilayer deposition can be carried out by immersing the substrate into the cationic and anionic solutions, alter- nately. After deposition of each layer, the substrate is immersed into the washing solution. Both adsorption steps can be repeated cyclically to form multilayer structures on the su