年产一万吨生物质基防冻液的生产工厂的工艺设计-学位论文.doc

长春工业大学学士毕业论文 PAGE  PAGE II 中文摘要 针对目前我国防冻液紧缺以及防冻液的质量不能满足现实的要求等问题，本设计提出基于以葡萄糖为原料经加氢制备的产物为基础来生产生物质基防冻液， 本设计进行了年产一万吨生物质基防冻液的生产工厂的工艺设计。 设计包括生物质基产品的介绍，防冻液的配置原理，工厂内的能量衡算，物料衡算，反应釜的计算与选型，离子交换器的计算与选型，确定了反应釜的体积为7.65m3 ，离子交换器中阳树脂高度和阴树脂高度。并且介绍了工厂的整体布局原则以及车间设计的相关内容，绘制了车间布置图，工艺流程图，反应釜装配图。 关键词：防冻液 反应釜 离子交换器 车间布置 工艺设计 Abstract Nowadays, our country faces the problems of shortage of antifreezer and the poor quality of antifreezer. In order to solve these problems, the thesis is based on the principle of the glucose as raw material to generate biomass-based antifreezer with the reaction of hydrogenation. The thesis is something about a factory process design of an annual output of ten thousand tons of antifreezer. The thesis includes the introduction of biomass-based products ，the principle of the preparation of antifreezer, the energy calculation of factory, the material balance calculations, the calculation and selection of the reactor, the calculation and selection of ion exchanger. Finally I determine the volume of the reactor for 7.65 m3 and the height of cationic resin and anion resin that filled in the ion exchanger .And then the thesis introduces the principle and the overall layout of the workshop design and in the thesis I draw the workshop layout and process diagram, the reactor assembly drawing. Key words: antifreeze the reactor ion exchanger workshop layout process design  目录  TOC \o 1-3 \u 第一章 文章的综述  PAGEREF _Toc327642425 \h 1 1.1 选题的背景  PAGEREF _Toc327642426 \h 1 1.2 生物质基产品的工业意义  PAGEREF _Toc327642427 \h 2 1.3设计依据的技术说明：  PAGEREF _Toc327642428 \h 5 1.3.1 生物质基防冻液母液的生产原理  PAGEREF _Toc327642429 \h 6 1.3.2 制备葡萄糖基防冻液的反应机理  PAGEREF _Toc327642430 \h 6 1.3.3 生物质基防冻液制备过程  PAGEREF _Toc327642431 \h 6 1.3.4 主要原料性质及来源  PAGEREF _Toc327642432 \h 7 1.3.5主要实验装置  PAGEREF _Toc327642433 \h 8 1.3.6 实验结果与讨论  PAGEREF _Toc327642434 \h 8 1.4 中试制备过程  PAGEREF _Toc327642