Perchloric acid - nitric acid digestion - atomic fluorescence spectrometry and Pieces Cynomorium lead content.doc

 PAGE \* MERGEFORMAT 9 Perchloric acid - nitric acid digestion - atomic fluorescence spectrometry and Pieces Cynomorium lead content [Abstract] Objective To establish a high-acid - nitric acid digestion - atomic fluorescence spectrometry and Pieces Cynomorium lead content. Methods by perchloric acid - nitric acid digestion, by atomic fluorescence spectrometry of trace lead content Cynomorium. The results of lead concentration in the 0.00 ~ 10.00 ng / mL and the fluorescence intensity within the linear relationship, linear equation: Y = 408.459 3X-72.159 5, r = 0.999 5. sample 6 determined the relative standard deviation 2.8%, recovery was 93.7% to 96.0%. Conclusion The method is simple, rapid, accurate, reproducible and satisfactory results. [Keywords:] perchloric acid - nitric acid digestion; atomic fluorescence spectrometry; Cynomorium; lead content; Abstract: Objective To establish the method of determining the content of lead in Cynomorium Songaricum Rupr. By atomic fluorescen spectrometry. Method After digested by perchloric acid-nitric acid, atomic fluorescen spectrometry was used to determining the content of lead in Cynomorium Songaricum Rupr .. Results When the concentration of trace lead was 0.00 ~ 10.00 ng / mL, it had linear relationship with fluorescence intensity. The linear function was Y = 408.459 3X-72.159 5, and the linear correlation coefficient was 0.999 5. The relative standard deviation of six determination results of the samples was 2.8%. The recovery rate was 93.7% ~ 96.0%. Conclusion The method is featured by easy operation, fast speed and good sensitivity. Keywords:: digested by perchloric acid-nitric acid; atomic fluorescen spectrometry method; Cynomorium songaricum Rupr.; Trace lead; content determination At present, the international response to the determination of heavy metals in traditional Chinese medicine attaches great importance to many countries on imported heavy metals in Chinese herbal medicines have clear l