Qi Pills Yangyinjiangtang Determination of Astragaloside.docVIP

 PAGE \* MERGEFORMAT 7 Qi Pills Yangyinjiangtang Determination of Astragaloside Author: Yan Suqin, Lixiang Yong, Song Xiaolin [Keywords:] Yiqiyangyin hypoglycemic pills;,, TLC;,, astragaloside Abstract: Objective To establish a hypoglycemic pills Yiqiyangyin Astragaloside method for the determination. Methods dual-wavelength reflection zigzag scanning method λ s = 530 nm, λ R = 700 nm. Results Qi Pills Yangyinjiangtang average concentration of Astragaloside 0.09%, the average recovery was 97.4%, RSD = 2.1%, the linear equation Y = 628.499 143.288 X (r = 0.999 8, n = 5). Conclusion This method can be used as hypoglycemic pills Yiqiyangyin quality control methods. Keywords:: Yiqi Yangyinjiangtang pill; TLC scanning; Astragaloside Qi Yangyinjiangtang pill for the newly developed compound preparation of Chinese medicine treatment of diabetes by more than 10 Chinese herbal medicines such as astragalus composition, clinical use good effect, in which Astragalus King and medicine, but as Astragalus astragaloside the main active ingredients, Therefore, in order to Astragaloside as an index to measure its content of the sample, to establish the preparation method for the determination. 1 Materials and equipment 1.1 Instrument Shimadzu CS9000 dual-wavelength flying spot scanner, TLC, TLC spotting Taiwan (Xian Qin West Machinery Factory), micro-injector (Ningbo Zhenhai glass instrument factory). 1.2 Test drug chromatography on silica gel G (Jimo, Shandong Chemical Reagent Factory) and the remaining reagents were analytical pure: astragaloside, purchased from China Pharmaceutical and Biological Products Institute (781-9002); Qi Yangyinjiangtang pill (in this House-made). 2 Methods and Results 2.1 Preparation of Solution 2.1.1 Preparation of precision control drug solution, said to take 105 ℃ drying to constant weight Astragaloside reference standards, using methanol produced about 1.0 mg per ml of solution, as a reference substance solution. 2.1.2 Preparation f