- 1、本文档共8页,可阅读全部内容。
- 2、原创力文档(book118)网站文档一经付费(服务费),不意味着购买了该文档的版权,仅供个人/单位学习、研究之用,不得用于商业用途,未经授权,严禁复制、发行、汇编、翻译或者网络传播等,侵权必究。
- 3、本站所有内容均由合作方或网友上传,本站不对文档的完整性、权威性及其观点立场正确性做任何保证或承诺!文档内容仅供研究参考,付费前请自行鉴别。如您付费,意味着您自己接受本站规则且自行承担风险,本站不退款、不进行额外附加服务;查看《如何避免下载的几个坑》。如果您已付费下载过本站文档,您可以点击 这里二次下载。
- 4、如文档侵犯商业秘密、侵犯著作权、侵犯人身权等,请点击“版权申诉”(推荐),也可以打举报电话:400-050-0827(电话支持时间:9:00-18:30)。
查看更多
RP-HPLC on the bone content of ferulic acid capsules_0
PAGE \* MERGEFORMAT 8
RP-HPLC on the bone content of ferulic acid capsules
[Abstract] Objective To establish a bone capsule for determining the content of ferulic acid. Methods HPLC, column: Hypersil C18 (4.6 mm × 250 mm, 5 μm), mobile phase was methanol -1% ice acetic acid (33:67), detection wavelength was 320 nm, flow rate 1.0 mL / min. Results of ferulic acid in the range of 0.12 ~ 1.2 μg linear relationship (r = 0.999 9), the average recovery was 99.6% , RSD = 1.8%. Conclusion The method is simple, accurate, and can be used to control the quality of bone capsules.
Keywords:] bone capsule, ferulic acid, HPLC, determination
Abstract: Objective To establish a method for determination of Ferulic acid in Jiegu Capsule. Method The samples were determined by RP-HPLC on a Hypersil C18 column (4.6 mm × 250 mm, 5 μm). The mobile phase consisted of methanol and 1% acetic acid (33:67). The detection wavelength was at 320 nm and the flow rate was 1.0 mL / min. Results The calibration curves of Ferulic acid was linear in the range of 6 ~ 60 μg / mL (r = 0.999 9) . The average recovery was 99.6% and RSD was 1.8%. Conclusion The method is simple and accurate, which can be used for the quality control of Jiegu Capsule.
Keywords:: Jiegu Capsule, Ferulic acid; HPLC, content determination
Capsule is in the bone pieces bone [“Chinese Ministry of Health, prescription drug standard preparation” (Volume 2) WS3-B-0402-90] based on the development of new agents, by the fourth copper, Chuan Xiong, Radix system , angelica, frankincense (vinegar Sunburn), myrrh (vinegar Sunburn), native copper (calcined) composed of 7 herbs, with stasis, promoting blood circulation, analgesic efficacy, clinical for traumatic injury, tendon injury fractures, bleeding sore . ferulic acid-based products one of the active ingredient, and higher levels. This test uses high performance liquid chromatography in the bone capsule of the determination of ferulic acid, to control the quality of t
您可能关注的文档
- Rivers and lakes of the joint recruitment of exotic forest.doc
- Rivers and mountains of tea to be the revitalization of the country re.doc
- Rivers and lakes roots - Inner Mongolia Yao Jiaohui.doc
- Rivets suture treatment of medial collateral ligament injury of starting and ending point of the Ministry of grade.doc
- Risperidone in the treatment of depression status.doc
- RMB appreciation export companies how to respond-.doc
- RMB appreciation is painful for the electronics industry good.doc
- RMB exchange rates against the impact of China's import and export trade.doc
- Rituximab 1 case report of adverse reactions and nursing.doc
- RNA interference Bcl2 expression in human gallbladder carcinoma cell line GBCSD of tumor growth in nude mice.doc
- 智云数码稳定器ZHIYUN CINEPEER WEEBILL 3E Guía del usuario说明书用户手册(语言:Español).pdf
- 信息化保障总结汇报.pptx
- 水产养殖技术总结汇报.pptx
- Siemens西门子工业SITRANS LR500 系列 (mA HART) SITRANS LR500 系列 (mA HART)使用手册.pdf
- 艺术类专业总结汇报.pptx
- 数学作业设计总结汇报.pptx
- Siemens西门子工业SIMATIC 分布式 I O SIMATIC Compact Field Unit (CFU) CIO HART SIMATIC 分布式 I O SIMATIC Compact Field Unit (CFU) CIO HART使用手册.pdf
- 辅导员周总结汇报.pptx
- ABB Open closed auxiliary contacts 6Q for fixed circuit-breaker 手册(英语)说明书.pdf
- 体育系年终总结汇报.pptx
文档评论(0)