直接电化学还原钛合金固体氧化物熔盐剖析.pptx

朱诗悦 李一航 王亚光 张璐 宦道明 程涛 夏飞 倪 堃 杨明晔 武煜森;Ti;The conventional methods ;Direct electrochemical reduction;FFC;Advatages of FFC;Alloy;Fig. 1. The phase diagram of Ti–Si system;Fig. 2. XRD patterns of the mixed powders (TiO2:SiO2 = 5:3) electrolyzed for different times. (a) 1 h; (b) 3 h; (c) 5 h.;Fig. 3. SEM images of the cross-section of a mixed powder pellet (TiO2:SiO2 = 5:3) electrolyzed for 3 h. (a) The whole pellet; (b) the inner part of the pellet; (c) the boundary of inner and outer parts; (d) the outer part. The inset plots in (b) and (d) are the EDX spectra measured over the image areas, respectively.;Fig. 4. The current–time curves of the electrolysis for different time, TiO2:SiO2 = 5:3, the insert is the initial part of the current–time curve.;Fig. 5. The SEM images of the products completely electrolyzed (electrolyzed for 5 h) with different starting stoichiometries: (a) TiO2:SiO2 = 3:1; (b) TiO2:SiO2 = 5:3; (c) TiO2:SiO2 = 5:4; (d) TiO2:SiO2 = 1:1; (e) TiO2:SiO2 = 1:2.;conclusion;Thank you! Happy new year!