Novel Poly-Dopamine Adhesive for a Halloysite Nanotube-Ru(bpy)32+ Electrochemiluminescent Sensor 英文参考文献.docVIP
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NovelPoly-DopamineAdhesiveforaHalloysiteNanotube-Ru(bpy)32ElectrochemiluminescentSensor英文参考文献
NovelPoly-DopamineAdhesiveforaHalloysite
Nanotube-Ru(bpy)32+ElectrochemiluminescentSensor
BoXing,Xue-BoYin*
ResearchCenterforAnalyticalSciences,CollegeofChemistry,NankaiUniversity,Tianjin,People’sRepublicofChina
Abstract
Herein,forthefirsttime,theelectrochemiluminescentsensorbasedonRu(bpy)32+-modifiedelectrodeusingdopamineas
anadhesivewassuccessfullydeveloped.Afterhalloysitenanotubeslurrywascastonaglassycarbonelectrodeanddried,an
alkalinedopaminesolutionwasaddedontheelectrodesurface.Initially,polydopaminebeltswithdimensionsoftensto
hundredsofnanometersformedviaoxidizationofthedopaminebyambientoxygen.Astheincubationtimeincreased,the
nanobeltsbecamebroaderandthenunitedwitheachothertoformapolydopaminefilm.Thehalloysitenanotubeswere
2+
embedded within the polydopamine film. The above electrode was soaked in Ru(bpy)3 aqueous solution to adsorb
2+
Ru(bpy)3 intotheactivesitesofthehalloysitenanotubesviacation-exchangeprocedure.Throughthissimpleprocedure,a
Ru(bpy)3 -modified electrode was obtained using only 6.25mg Ru(bpy)3 , 15.0 g dopamine, and 9.0mg halloysite
nanotubes. The electrochemistry and electrochemiluminescence (ECL) of the modified electrode was investigated using
tripropylamine(TPA)andnitrilotriaceticacid(NTA)asco-reactants.ThedifferentECLbehaviorsofthemodifiedelectrode
usingNTAandTPAaswellasthecontactanglemeasurements reflectedthehydrophilic characteroftheelectrode.The
2+
2+
m
2+
resultsindicatethathalloysitenanotubeshaveahighloadingcapacityforRu(bpy)3 andthatdopamineissuitableforthe
preparationofmodifiedelectrodes.
Citation:XingB,YinX-B(2009)NovelPoly-DopamineAdhesiveforaHalloysiteNanotube-Ru(bpy)32+ElectrochemiluminescentSensor.PLoSONE4(7):e6451.
doi:10.1371/journal.pone.0006451
Editor:CameronNeylon,UniversityofSouthampron,UnitedKingdom
ReceivedApril20,2009;AcceptedJune25,2009;PublishedJuly30,2009
Copyright:?2009Xing,Yin.Thisisanopen-accessarticledistributedunderthetermsoftheCreativeCommonsAttributionLicense,whichpermitsunrestricted
use,distr
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