化学英语实验报告.doc

化学英语实验报告 篇一：英文版化学实验报告 Preparation of ethyl acetate First, the purpose of the experiment: 1、 Learn from the general principles of organic synthetic esters and methods 2、 Master distillation, extraction, drying and other experimental techniques and its application in a specific experiment Second, the experimental principle: Main reaction： CH3COOH+CH3CH2OH=CH3COOCH2CH3+H2O Conditions: heating to 120 to 125 °C in concentrated sulfuric acid catalyzed Side effects ： 浓H2SO4 CH3CH2OH---------gt;CH2=CH2+H2O 170度 浓H2SO4 CH3CH2OH---------gt;CH3CH2OCH2CH3+H2O 140度 Third, the instruments and reagents: 1、 Instruments and materials: Round-bottomed flask, Spherical condenser, Straight condenser，Distillation head, a separatory funnel, measuring beakers, dropper, conical flask, thermometer, electric 2、 drugs: Glacial acetic acid (AR), absolute ethanol (AR), concentrated sulfuric acid, saturated brine, a saturated sodium carbonate solution, a saturated calcium chloride solution, dried over anhydrous magnesium sulfate, litmus Fourth,Reactor： Fifth,Experimental procedure: Adding 50ml round bottom flask 3ml 5ml ethanol and acetic acid, in shaking batch of concentrated sulfuric acid was added 1.3ml mixed, and add a few grains of zeolite, and then install the instrument response Low heat, slowly reflux for 30 minutes. Coolish, reflux device to the distillation apparatus, wetted with cold water to cool the bottle. Heating distillation until the distillate liquid volume is about half the volume of the reaction so far to give the crude product in ethyl acetate The distillate was slowly saturated sodium carbonate solution was added portionwise, and oscillate until the evolution of carbon dioxide gas without using litmus paper test acetate layer was neutral. The mixture was then transferred to a separatory funnel, and separated aqueous layer was washed once with saturated aqueous saline solution 3ml The organic layer was washed with a saturated solution of calcium c