WC对原位合成Mo2FeB2烧结及组织性能的影响.pdfVIP

学兔兔 第27卷第3期 粉末冶金技术 Vo1．27，No．3 2OO9年6月 Powder Metallurgy Technology Jun．2009 WC对原位合成Mo2 FeB2烧结 及组织性能的影响 李文虎 刘福田 1)(陕西理工学院材料科学与工程学院，陕西汉中 723003) 2)(济南大学材料科学与工程学院，济南 250022) 摘 要： 在Mo—B·Fe-Cr-Ni系统中，分别掺加不同含量的WC进行真空液相烧结，用电子万能材料试验机和硬度计 测定材料的弯曲强度与硬度，用XRD、SEM观察分析材料的物相和组织结构。结果表明，在满足反应生成Mo FeB： 的前提下，掺加的WC作为形核中心，降低了烧结过程中的成核位垒，使烧结过程更易进行，烧结生成的Mo FeB 硬 质相与WC晶粒形成了无污染、弱界面结合的双硬质相，并且在粘结相中分布均匀，提高了材料的抗弯强度和硬度。 关键词：原位反应；烧结；Me2FeB2 Effect of WC content on sinteidng process and structure properties for in situ sintering synthesis of Mo2FeB2 Li Wenhu )． Liu Futian2) ， 1)(School of Material Science and Engineering，Shanxi University of Technology，Hanzhong Shanxi 723003，China) 2)(School of Material Science and Engineering，Ji nan University，ji nan 250022，China) Abstract：In-situ Mo2 FeB2 material was obtained by adding different contents of WC in Mo-B ·Fe·Cr·Ni system and carrying out the vacuum sintering．The bending strength and hardness were tested by electronic universal material testing machine and hard ometa1．The phase and microstructure of the material were analyzed by means of XRD and SEM．The results show that in on the condition of preparing the Mo2 FeB2，the extra WC as the nucleation centre will reduce nucleation barrier during sintering process．The pollution-free and weak interface bonding composite carbide