Sn-16%Sb包晶合金的定向凝固组织演化研究.pdfVIP

维普资讯 学兔兔 May2008 VO1．57 NO．5 Sn一1 6％Sb包晶合金的定向凝固组织演化研究 胡小武，李双明，刘 林，傅恒志 (西北工业大学凝固技术国家重点试验室，陕西西安710072) 摘要：利用高温度梯度定向凝固装置对Sn一16wt．％Sb过包晶合金进行了试验研究，考察了不同凝固速度条件下获得的 凝固组织、相的形貌及初生相体积分数的变化。结果表明，定向凝固组织为硬质初生金属间化合物SnSb相弥散分布于 包晶13(Sn)相的软基体中，SnSb相呈四方形或三角形状，呈现小平面相生长形态。同时发现初生相随定向凝固速率增 大而细化，分布更加均匀，其体积分数随定向凝固速率的增大先减小后增大。 关键词：Sn．16％Sb包晶合金；定向凝固；初生相；形态尺度；体积分数 中图分类号：TGI 14．4 文献标识码：A 文章编号：1001—4977(2008)05—0446—05 Microstructures Evolution of Directionally Solidified Sn一1 6％Sb Hyperperitectic Alloy HU Xiao—WU，LI Shuang—ming，LIU Lin，FU Heng—zhi (State Key Laboratory of Solidification Processing，Northwestern Polytechnical University Xi’an 71 0072，Shaanxi，China) Abstract： Directional solidified microstructures of Sn一1 6％Sb hyperpe ritectic alloy have been investigated at various solidification rates using a high—thermal gradient directional solidification apparatus．The results 1ndicate that the solidification microstructures consist of hard primary intermetallic SnSb phase embedded in a matrix of soft peritectic 3-Sn phase．The primary SnSb phase exhibits the faceted growth with the tetragonal or trigonal shapes．At the same time，the primary SnSb phase iS refined with the increase of the solidification rate and dispersed more uniformlv in the matrix of 13 Sn phase．The volume fraction of SnSb phase firstly decrease and then increase．when the sOlidmcatiOn rate increases in directional solidification of Sn．1 6