耐火浇注料的研制与性能检测(国外英文资料).docVIP

耐火浇注料的研制与性能检测(国外英文资料) 160.3 160.8 160.7 L1 160.1 160.2 160.6 The line rate Δ Lh = (L1 - L0)/L1 * 100 0.06 0.12 0.12 Test the porosity and volume density of the sample Porosity: the ratio of the volume of all open pores in the porous material to the total volume of the open pores in the porous material. Bulk density refers to the quality of the porous materials and the ratio of total volume, ɡ / ㎝ 3. Principle: to measure the dry mass of the specimen, and to measure the volume of the sample by using the liquid static, and calculate the porosity and volume density. Equipment: electric and hot drying cabinet; Vacuuming device; Container with overflow pipe; Balance; towel Experimental steps 1) sample request: each group of samples shall not be less than 3 pieces, volume for ㎝ 3, 100-200, the ratio of the longest and shortest while no more than 2:1. 2) dry sample weighing: first brush sample surface adhesion of finely granular net, in the electric heating oven at 110 + 5 ℃ drying after two hours, and in the natural cooling to room temperature in the oven. The mass of each specimen is recorded as m1 and is accurate to 0.01 g. 3) sample dipping: put in the sample container, as for the vacuum device, the vacuum to the residual stress is less than 2.5 KPa, keep constant pressure for 5 min, then within 5 min slow infusion liquid, until the sample completely submerged. Keep 30min in vacuum to fully saturate the sample. 4) of saturated specimen apparent quality measurement: remove the saturated samples quickly to take the overflow pipe in the container, on the hook of the scale, need completely submerged impregnation liquid sample and in the page after the calm, weighing suspended in the liquid saturation specimen quality, as m2. Accurate to 0.01 g. 5) of saturated specimen quality measurement: from the pickling liquid sample, the use of saturated liquid towel, carefully wipe the specimen surface to excess liquid droplets (not suck out the porosity of the liquid). Immediately